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reaction temperature and mixing conditions in case of an in-situ polymerized nanocomposite. Figure 2. illustrates two examples of transmission electron microscopy (TEM) images taken from highly intercalated or orderly exfoliated epoxy nanocomposites. The general requirements to achieve the formation of epoxy nanocomposites were established by the group of Pinnavaia et al. In brief, the nature of the layered silicate and the interlayer exchanged ion, the cure conditions and the resin and hardener chemistry are the key factors controlling the final composite structure. Recent work by Park and Jana25 expanded on this process by noting that polymerizing networks may store up elastic energy, which pushes against the interacting clay layers, the mobility of the layers themselves inhibited by the viscosity of the reacting monomer sitting outside the clay layers at any given time. The force balance thus involves the attractive clay-organo-ion adhesion and, importantly, interaction between the organo-ions themselves, and is illustrated in Fig. 2. . Such a build-up in energy of the cure inside the gallery means that entropy increases to a point that this counterbalances the attractive energies and the clay expands. An important part of the understanding put forward is that the surface layers become removed first in a sequential manner, and that, in fact, they peel off from the edges because of the flexibility of the clay. Kong and Park26 added further to the understanding with some elegant, real- time X-ray diffraction studies, which allowed the monitoring of changes in d- spacing with reaction. They found that slower curing rates (due to less reactive amines as indicated by their electronegativities, pKa) or increased cure temperatures led to better exfoliation. It was found for the system investigated that the d-spacing occurs at a certain point (after approximately 9 minutes, see Fig. 2. ) when a sudden peak at 3. nm occurs. This indicates that the change in d-spacing can occur quite quickly and that simple diffusion alone of monomer into the galleries is not sufficient to push the clay apart, but rather that the elastic build-up described above by Park and Jana25 is required. Indeed, three step- 2. Relationship between storage modulus and viscosity as a function of curewith the standard epoxy resin (glycidyl ether of bisphenol A) with JeffamineD230 (denoted P in the legend) or with DDS (denoted D in the legend).

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